2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole

Base Information

Chemical Name:2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole
CAS No.:1570494-02-8
Molecular Formula:C₁₇H₁₃ClN₆O
Molecular Weight:352.783
Hs Code.:

Synonyms:2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole

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Chemical Property of 2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole

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Technology Process of 2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole

There total 2 articles about 2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 101990-73-2
2-chloro-pyridin-4-ylmethyl chloride

: 1570493-99-0
2-(5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole

: 1570494-02-8
2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole

Guidance literature:: With caesium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 99367-59-6
5-phenyl-1,3,4-oxadiazole-2-carbohydrazide

: 1570494-02-8
2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / 5,5-dimethyl-1,3-cyclohexadiene / 36 h / 170 °C

2: caesium carbonate; sodium iodide / N,N-dimethyl-formamide / 20 °C

With caesium carbonate; sodium iodide; sodium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; N,N-dimethyl-formamide;

Reference yield: 27.0%

: 1570494-02-8
2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole

: 38646-68-3
4,4-dimethylpiperidine hydrochloric acid salt

: 76-05-1
trifluoroacetic acid

: 1570493-97-8
2-(4,4-dimethylpiperidin-1-yl)-4-((5-methyl-3-(5-phenyl-1,3,4-oxadiazol-2-yl)-1H-1,2,4-triazol-1-yl)methyl)pyridin-1-ium trifluoroacetate

Guidance literature:: 2-(1-((2-chloropyridin-4-yl)methyl)-5-methyl-1H-1,2,4-triazol-3-yl)-5-phenyl-1,3,4-oxadiazole; 4,4-dimethylpiperidine hydrochloric acid salt; With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 120 ℃;

trifluoroacetic acid; In water; acetonitrile;