dimethyl 1-cyclohexylidenemethylene-2-(tetrahydro-2H-pyran-2-yloxy)-propanephosphonate

Base Information

Chemical Name:dimethyl 1-cyclohexylidenemethylene-2-(tetrahydro-2H-pyran-2-yloxy)-propanephosphonate
CAS No.:1637401-59-2
Molecular Formula:C₁₇H₂₉O₅P
Molecular Weight:344.388
Hs Code.:

Synonyms:dimethyl 1-cyclohexylidenemethylene-2-(tetrahydro-2H-pyran-2-yloxy)-propanephosphonate

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Chemical Property of dimethyl 1-cyclohexylidenemethylene-2-(tetrahydro-2H-pyran-2-yloxy)-propanephosphonate

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Technology Process of dimethyl 1-cyclohexylidenemethylene-2-(tetrahydro-2H-pyran-2-yloxy)-propanephosphonate

There total 2 articles about dimethyl 1-cyclohexylidenemethylene-2-(tetrahydro-2H-pyran-2-yloxy)-propanephosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₁₇H₂₉O₄P

: 1637401-59-2
dimethyl 1-cyclohexylidenemethylene-2-(tetrahydro-2H-pyran-2-yloxy)-propanephosphonate

Guidance literature:: In diethyl ether; at -70 - 20 ℃; for 11h;
DOI:10.3390/molecules19056309

Reference yield:

: 1637401-51-4
1-[3-(tetrahydro-2H-pyran-2-yloxy)-but-1-ynyl]-cyclohexanol

: 1637401-59-2
dimethyl 1-cyclohexylidenemethylene-2-(tetrahydro-2H-pyran-2-yloxy)-propanephosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus trichloride; triethylamine / diethyl ether / 0.5 h / -70 °C

2: diethyl ether / 11 h / -70 - 20 °C

With triethylamine; phosphorus trichloride; In diethyl ether;
DOI:10.3390/molecules19056309