(S)-tert-butyl 3-(4-chlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate

Base Information

Chemical Name:(S)-tert-butyl 3-(4-chlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate
CAS No.:1231958-23-8
Molecular Formula:C₁₈H₂₄ClNO₃
Molecular Weight:337.846
Hs Code.:

Synonyms:(S)-tert-butyl 3-(4-chlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate

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Chemical Property of (S)-tert-butyl 3-(4-chlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate

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Technology Process of (S)-tert-butyl 3-(4-chlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate

There total 3 articles about (S)-tert-butyl 3-(4-chlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1231958-22-7
(S)-tert-butyl 3-(4-chlorophenyl)-3-(2-hydroxyethyl)piperidine-1-carboxylate

: 1231958-23-8
(S)-tert-butyl 3-(4-chlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate

Guidance literature:: With pyridine-SO₃ complex; triethylamine; In dimethyl sulfoxide; at 25 ℃; for 0.333333h; Cooling; Inert atmosphere;

Reference yield:

: 1231956-18-5
(S)-2-(3-(4-chlorophenyl)piperidin-3-yl)ethanol

: 1231958-23-8
(S)-tert-butyl 3-(4-chlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 18 h / 25 °C / Inert atmosphere

2: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 0.33 h / 25 °C

With sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; dimethyl sulfoxide;

Reference yield:

: 1232237-09-0
(S)-(-)-2-(3-(3,4-dichloro-phenyl)-piperidine-3-yl)ethanol

: 1231958-23-8
(S)-tert-butyl 3-(4-chlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride; methanol / diethyl ether; tetrahydrofuran / 48 h / 20 °C / Inert atmosphere

2: tetrahydrofuran / 18 h / 25 °C / Inert atmosphere

3: triethylamine; sulfur trioxide pyridine complex / dimethyl sulfoxide / 0.33 h / 25 °C

With methanol; lithium aluminium tetrahydride; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide;