8-azido-N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine

Base Information

• Chemical Name: 8-azido-N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine
• CAS No.: 328241-05-0
• Molecular Formula: C₂₆H₃₄N₈O₅Si
• Molecular Weight: 566.692

Synonyms:8-azido-N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine

Chemical Property of 8-azido-N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine

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Technology Process of 8-azido-N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine

There total 1 articles about 8-azido-N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

N6-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine (292642-43-4) → 8-azido-N6-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine (328241-05-0)

Guidance literature:

With 4-toluenesulfonyl azide; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1.25h;

DOI:10.1002/1522-2675(20001220)83:12<3229::AID-HLCA3229>3.0.CO;2-S

Reference yield: 91.0%

8-azido-N6-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine (328241-05-0) → 8-amino-N6-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine (328241-06-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; at 25 ℃; for 4h;

DOI:10.1002/1522-2675(20001220)83:12<3229::AID-HLCA3229>3.0.CO;2-S

Reference yield: 45.0%

8-azido-N6-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine (328241-05-0) + trimethylsilylacetylene (1066-54-2) → N6-benzoyl-2',3'-O-isopropylidene-8-(1H-[1,2,3]triazol-1-yl)-5'-O-(triethylsilyl)adenosine

Guidance literature:

In N,N-dimethyl-formamide; at 80 ℃; for 20h;

DOI:10.1002/1522-2675(20001220)83:12<3229::AID-HLCA3229>3.0.CO;2-S

upstream raw materials:

N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine

Downstream raw materials:

8-amino-N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine

N⁶-benzoyl-8-iodo-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosine

N⁶-benzoyl-2',3'-O-isopropylidene-5'-O-(triethylsilyl)adenosin-8-yl-(8->7)-8-amino-N⁶-benzoyl-9-[6,7-dideoxy-2,3-O-isopropylidene-5-O-(triethylsilyl)-β-D-allo-hept-6-ynofuranosyl]adenine

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