N,N'-[2,5-bis(4-oxidomorpholin-4-yl)-1,4-phenylene]diacetamide

Base Information

Chemical Name:N,N'-[2,5-bis(4-oxidomorpholin-4-yl)-1,4-phenylene]diacetamide
CAS No.:1374780-52-5
Molecular Formula:C₁₈H₂₆N₄O₆
Molecular Weight:394.428
Hs Code.:

Synonyms:N,N'-[2,5-bis(4-oxidomorpholin-4-yl)-1,4-phenylene]diacetamide

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Chemical Property of N,N'-[2,5-bis(4-oxidomorpholin-4-yl)-1,4-phenylene]diacetamide

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Technology Process of N,N'-[2,5-bis(4-oxidomorpholin-4-yl)-1,4-phenylene]diacetamide

There total 6 articles about N,N'-[2,5-bis(4-oxidomorpholin-4-yl)-1,4-phenylene]diacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1374780-44-5
N,N'-[2,5-di(morpholin-4-yl)-1,4-phenylene]diacetamide

: 1374780-52-5
N,N'-[2,5-bis(4-oxidomorpholin-4-yl)-1,4-phenylene]diacetamide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In acetone; for 1h; Reflux;
DOI:10.1002/ejoc.201101687

Reference yield:

: 398-90-3
(2,5-difluorophenyl)acetanilide

: 1374780-52-5
N,N'-[2,5-bis(4-oxidomorpholin-4-yl)-1,4-phenylene]diacetamide

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid; nitric acid / 1 h / 0 °C

2: methanesulfonic acid; dihydrogen peroxide / 2 h / 55 °C

3: sodium hydrogencarbonate / tetrahydrofuran / 3 h / 50 °C

4: 5%-palladium/activated carbon; hydrogen / acetic acid / 16 h / 20 °C / 4500.45 Torr

5: 3-chloro-benzenecarboperoxoic acid / acetone / 1 h / Reflux

With methanesulfonic acid; sulfuric acid; 5%-palladium/activated carbon; hydrogen; dihydrogen peroxide; nitric acid; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; acetic acid; acetone;
DOI:10.1002/ejoc.201101687

Reference yield:

: 367-30-6
2,5-difluoroaniline

: 1374780-52-5
N,N'-[2,5-bis(4-oxidomorpholin-4-yl)-1,4-phenylene]diacetamide

Guidance literature:: Multi-step reaction with 6 steps

1: methanol / 0.5 h / 20 °C

2: sulfuric acid; nitric acid / 1 h / 0 °C

3: methanesulfonic acid; dihydrogen peroxide / 2 h / 55 °C

4: sodium hydrogencarbonate / tetrahydrofuran / 3 h / 50 °C

5: 5%-palladium/activated carbon; hydrogen / acetic acid / 16 h / 20 °C / 4500.45 Torr

6: 3-chloro-benzenecarboperoxoic acid / acetone / 1 h / Reflux

With methanesulfonic acid; sulfuric acid; 5%-palladium/activated carbon; hydrogen; dihydrogen peroxide; nitric acid; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; acetic acid; acetone;
DOI:10.1002/ejoc.201101687