ethyl (E)-5,5-bis[(benzyloxy)methyl]-8-(N,N-diethylcarbamoyl)-2-octen-7-ynoate

Base Information

Chemical Name:ethyl (E)-5,5-bis[(benzyloxy)methyl]-8-(N,N-diethylcarbamoyl)-2-octen-7-ynoate
CAS No.:1078789-47-5
Molecular Formula:C₃₁H₃₉NO₅
Molecular Weight:505.654
Hs Code.:

Synonyms:ethyl (E)-5,5-bis[(benzyloxy)methyl]-8-(N,N-diethylcarbamoyl)-2-octen-7-ynoate

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Chemical Property of ethyl (E)-5,5-bis[(benzyloxy)methyl]-8-(N,N-diethylcarbamoyl)-2-octen-7-ynoate

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Technology Process of ethyl (E)-5,5-bis[(benzyloxy)methyl]-8-(N,N-diethylcarbamoyl)-2-octen-7-ynoate

There total 4 articles about ethyl (E)-5,5-bis[(benzyloxy)methyl]-8-(N,N-diethylcarbamoyl)-2-octen-7-ynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374149-01-5
C₃₁H₄₃NO₅

: 1078789-47-5
ethyl (E)-5,5-bis[(benzyloxy)methyl]-8-(N,N-diethylcarbamoyl)-2-octen-7-ynoate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / Inert atmosphere

2: sodium hydride / Inert atmosphere

With sodium hydride; toluene-4-sulfonic acid;
DOI:10.1021/ol300623j

Reference yield:

: 2-(2,2-diethoxyethyl)-2-prop-2-ynylmalonic acid diethyl ester

: 1078789-47-5
ethyl (E)-5,5-bis[(benzyloxy)methyl]-8-(N,N-diethylcarbamoyl)-2-octen-7-ynoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium tetrahydride / Inert atmosphere

2.1: sodium hydride / Inert atmosphere

2.2: Inert atmosphere

3.1: n-butyllithium / Inert atmosphere

3.2: Inert atmosphere

4.1: toluene-4-sulfonic acid / Inert atmosphere

5.1: sodium hydride / Inert atmosphere

With lithium aluminium tetrahydride; n-butyllithium; sodium hydride; toluene-4-sulfonic acid;
DOI:10.1021/ol300623j

Reference yield:

: 1374148-99-8
C₁₂H₂₂O₄

: 1078789-47-5
ethyl (E)-5,5-bis[(benzyloxy)methyl]-8-(N,N-diethylcarbamoyl)-2-octen-7-ynoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / Inert atmosphere

1.2: Inert atmosphere

2.1: n-butyllithium / Inert atmosphere

2.2: Inert atmosphere

3.1: toluene-4-sulfonic acid / Inert atmosphere

4.1: sodium hydride / Inert atmosphere

With n-butyllithium; sodium hydride; toluene-4-sulfonic acid;
DOI:10.1021/ol300623j