ethyl 3--amino-4-methyl-2-pentenoate

Base Information

Chemical Name:ethyl 3--amino-4-methyl-2-pentenoate
CAS No.:170745-53-6
Molecular Formula:C₁₆H₂₃NO₂
Molecular Weight:261.364
Hs Code.:

ethyl 3-<N-(R)-1-phenylethyl>-amino-4-methyl-2-pentenoate

Synonyms:ethyl 3--amino-4-methyl-2-pentenoate

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Chemical Property of ethyl 3--amino-4-methyl-2-pentenoate

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Technology Process of ethyl 3--amino-4-methyl-2-pentenoate

There total 1 articles about ethyl 3--amino-4-methyl-2-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 167467-27-8
[1,2-Dimethyl-prop-(Z)-ylidene]-((R)-1-phenyl-ethyl)-amine

: 105-58-8,76619-83-5
Diethyl carbonate

: 170745-53-6
ethyl 3--amino-4-methyl-2-pentenoate

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; for 2h; -80 deg C to rt;
DOI:10.1016/0040-4020(95)00476-O

Reference yield: 58.0%

: 170745-53-6
ethyl 3--amino-4-methyl-2-pentenoate

: 169214-05-5
(3S,αR)-ethyl 3--4-methylpentanoate

: (3R,αR)-ethyl 3--4-methylpentanoate

Guidance literature:: With sodium tris(acetoxy)borohydride; In acetic acid; acetonitrile; at 0 ℃; for 4h;
DOI:10.1021/jo960107y

Reference yield:

: 170745-53-6
ethyl 3--amino-4-methyl-2-pentenoate

: 142342-78-7
(S)-3-Amino-4-methyl-pentanoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / NaHB(OAc)3 / acetic acid; acetonitrile / 4 h / 0 °C

2: 81 percent / H₂ / Pd(OH)2/C / methanol; H₂O; acetic acid / Ambient temperature

With hydrogen; sodium tris(acetoxy)borohydride; palladium dihydroxide; In methanol; water; acetic acid; acetonitrile;
DOI:10.1021/jo960107y