1-deoxy-1-diphenylphosphoryl-2,3:5,6-di-O-isoprpylidene-1-(2-naphthylamino)-D-mannite

Base Information

• Chemical Name: 1-deoxy-1-diphenylphosphoryl-2,3:5,6-di-O-isoprpylidene-1-(2-naphthylamino)-D-mannite
• CAS No.: 1150659-76-9
• Molecular Formula: C₃₄H₃₈NO₆P
• Molecular Weight: 587.653
• Mol file: 1150659-76-9.mol

Synonyms:1-deoxy-1-diphenylphosphoryl-2,3:5,6-di-O-isoprpylidene-1-(2-naphthylamino)-D-mannite

Chemical Property of 1-deoxy-1-diphenylphosphoryl-2,3:5,6-di-O-isoprpylidene-1-(2-naphthylamino)-D-mannite

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-deoxy-1-diphenylphosphoryl-2,3:5,6-di-O-isoprpylidene-1-(2-naphthylamino)-D-mannite

There total 1 articles about 1-deoxy-1-diphenylphosphoryl-2,3:5,6-di-O-isoprpylidene-1-(2-naphthylamino)-D-mannite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

C22H27NO5 (1150659-71-4) + Diphenylphosphine oxide (4559-70-0) → 1-deoxy-1-diphenylphosphoryl-2,3:5,6-di-O-isoprpylidene-1-(2-naphthylamino)-D-mannite (1150659-76-9)

Guidance literature:

With pyridine; In chloroform; at 60 ℃; for 23 - 27h; Inert atmosphere;

DOI:10.1134/S1070428008080071

Reference yield:

1-deoxy-1-diphenylphosphoryl-2,3:5,6-di-O-isoprpylidene-1-(2-naphthylamino)-D-mannite (1150659-76-9) → 1-deoxy-1-diphenylphosphoryl-1-phenylamino-D-mannite

Guidance literature:

With water; Acidic conditions;

DOI:10.1134/S1070428008080071

upstream raw materials:

C₂₂H₂₇NO₅

Diphenylphosphine oxide