(2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester

Base Information

Chemical Name:(2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester
CAS No.:768370-07-6
Molecular Formula:C₁₇H₁₈N₂O₄
Molecular Weight:314.341
Hs Code.:

(2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1<i>H</i>-isoindol-4-yl)-carbamic acid benzyl ester

Synonyms:(2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester

Suppliers and Price of (2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester

Chemical Property:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester

There total 1 articles about (2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 930-88-1
N-methylmaleimide

: 123-73-9,4170-30-3
trans-Crotonaldehyde

: 621-84-1
O-benzyl carbamate

: 768370-07-6
(2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester

Guidance literature:: With toluene-4-sulfonic acid; In 1-methyl-pyrrolidin-2-one; at 120 ℃;
DOI:10.1515/znb-2004-0411

Reference yield: 68.0%

: 768370-07-6
(2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester

: 2257-85-4
4-amino-2-methyl-1H-isoindole-1,3(2H)-dione

Guidance literature:: palladium on activated charcoal; In Triethylene glycol dimethyl ether; at 140 ℃;
DOI:10.1515/znb-2004-0411

Reference yield:

: 768370-07-6
(2-methyl-1,3-dioxo-2,3,3a,4,7,7a-hexahydro-1H-isoindol-4-yl)-carbamic acid benzyl ester

: 521-31-3
5-amino-2,3-dihydrophthalazine-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / Pd/C / triethylene glycol dimethyl ether / 140 °C

2: 70 percent / hydrazine hydrate / 110 °C

With hydrazine hydrate; palladium on activated charcoal; In Triethylene glycol dimethyl ether;
DOI:10.1515/znb-2004-0411