Technology Process of C44H27N3O
There total 8 articles about C44H27N3O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
ethanol; water; toluene;
for 24h;
Reflux;
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
ethanol; water; toluene;
at 120 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / Reflux
2.1: triethyl phosphite / neat (no solvent) / 5 h / 150 °C
3.1: copper(l) iodide; potassium phosphate / toluene / 24 h / 100 °C
4.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C
4.2: 1 h / 20 °C
5.1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / Reflux
6.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / Reflux
With
potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; sodium carbonate; potassium carbonate; triethyl phosphite;
In
tetrahydrofuran; ethanol; hexane; water; toluene;