2-((p-chlorophenylaminosulfonyl)methyl)-5-((3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazole

Base Information

• Chemical Name: 2-((p-chlorophenylaminosulfonyl)methyl)-5-((3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazole
• CAS No.: 1595281-78-9
• Molecular Formula: C₂₅H₁₈Cl₂N₄O₆S₂
• Molecular Weight: 605.479

Synonyms:2-((p-chlorophenylaminosulfonyl)methyl)-5-((3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazole

Chemical Property of 2-((p-chlorophenylaminosulfonyl)methyl)-5-((3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazole

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Technology Process of 2-((p-chlorophenylaminosulfonyl)methyl)-5-((3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazole

There total 3 articles about 2-((p-chlorophenylaminosulfonyl)methyl)-5-((3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2-((p-chlorophenylaminosulfonyl)methyl)-5-((4',5'-dihydro-3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazoles (1595281-72-3) → 2-((p-chlorophenylaminosulfonyl)methyl)-5-((3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazole (1595281-78-9)

Guidance literature:

With chloranil; In 5,5-dimethyl-1,3-cyclohexadiene; Reflux;

DOI:10.1248/cpb.c13-00652

Reference yield:

(N-4-chlorophenylsulfamoyl)acetic acid hydrazide (67542-00-1) → 2-((p-chlorophenylaminosulfonyl)methyl)-5-((3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazole (1595281-78-9)

Guidance literature:

Multi-step reaction with 3 steps

1: trichlorophosphate / Reflux

2: chloroamine-T / methanol / Reflux

3: chloranil / 5,5-dimethyl-1,3-cyclohexadiene / Reflux

With chloroamine-T; chloranil; trichlorophosphate; In methanol; 5,5-dimethyl-1,3-cyclohexadiene;

DOI:10.1248/cpb.c13-00652

Reference yield:

[(Z)-2-(4-Chloro-phenyl)-ethenesulfonyl]-acetic acid → 2-((p-chlorophenylaminosulfonyl)methyl)-5-((3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazole (1595281-78-9)

Guidance literature:

Multi-step reaction with 3 steps

1: trichlorophosphate / Reflux

2: chloroamine-T / methanol / Reflux

3: chloranil / 5,5-dimethyl-1,3-cyclohexadiene / Reflux

With chloroamine-T; chloranil; trichlorophosphate; In methanol; 5,5-dimethyl-1,3-cyclohexadiene;

DOI:10.1248/cpb.c13-00652

upstream raw materials:

2-((p-chlorophenylaminosulfonyl)methyl)-5-((4',5'-dihydro-3'-phenyl-5'-(p-chlorophenyl)isoxazol-4'-ylsulfonyl)methyl)-1,3,4-oxadiazoles

(N-4-chlorophenylsulfamoyl)acetic acid hydrazide

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