(Z)-3-bromopropenoic acid 2-iodophenyl ester

Base Information

• Chemical Name: (Z)-3-bromopropenoic acid 2-iodophenyl ester
• CAS No.: 444890-81-7
• Molecular Formula: C₉H₆BrIO₂
• Molecular Weight: 352.954
• Mol file: 444890-81-7.mol

Synonyms:(Z)-3-bromopropenoic acid 2-iodophenyl ester

Chemical Property of (Z)-3-bromopropenoic acid 2-iodophenyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (Z)-3-bromopropenoic acid 2-iodophenyl ester

There total 1 articles about (Z)-3-bromopropenoic acid 2-iodophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(Z)-3-bromoacrylic acid (1609-92-3) + 2-Iodophenol (533-58-4) → (Z)-3-bromopropenoic acid 2-iodophenyl ester (444890-81-7)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/jo025659x

Reference yield: 49.0%

buta-1,3-diyn-1-ylcyclohexane + (Z)-3-bromopropenoic acid 2-iodophenyl ester (444890-81-7) → 9,10-bis(cyclohexylethynyl)-6H-dibenzo[b,d]pyran-6-one

Guidance literature:

With potassium carbonate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 80 ℃; for 1h;

DOI:10.1021/jo025659x

Reference yield:

phenylacetylene (536-74-3) + (Z)-3-bromopropenoic acid 2-iodophenyl ester (444890-81-7) → (Z)-5-Phenyl-pent-2-en-4-ynoic acid 2-iodo-phenyl ester

Guidance literature:

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; at 40 ℃; for 2h;

DOI:10.1021/jo025659x

upstream raw materials:

(Z)-3-bromoacrylic acid

2-Iodophenol