1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanone

Base Information

• Chemical Name: 1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanone
• CAS No.: 122899-32-5
• Molecular Formula: C₁₃H₁₄O₅
• Molecular Weight: 250.251

Synonyms:1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanone

Chemical Property of 1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanone

Chemical Property:

Purity/Quality:

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Technology Process of 1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanone

There total 1 articles about 1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

1-(2-methyl-5-phenyl-4,5-dihydrofuran-3-yl)ethanone (13463-61-1) → 1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanone (122899-32-5) + 1,6-Dimethyl-3-phenyl-2,7,8,9-tetraoxabicyclo<4.2.1>nonan-5-one (122763-37-5)

Guidance literature:

With ozone; In tetrachloromethane; Product distribution; other solvents, other temp.;

DOI:10.1021/ja00201a051

Reference yield:

1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanone (122899-32-5) → 1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanol (122899-36-9,122999-23-9)

Guidance literature:

With sodium tetrahydroborate; In methanol;

DOI:10.1021/ja00201a051

Reference yield:

1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanone (122899-32-5) → Acetic acid 3-acetoxy-3-oxo-1-phenyl-propyl ester (122899-33-6)

Guidance literature:

at 20 ℃;

DOI:10.1021/ja00201a051

upstream raw materials:

1-(2-methyl-5-phenyl-4,5-dihydrofuran-3-yl)ethanone

Downstream raw materials:

1-((1S,3S,5S)-1-Methyl-3-phenyl-2,6,7,8-tetraoxa-bicyclo[3.2.1]oct-5-yl)-ethanol

Acetic acid 3-acetoxy-3-oxo-1-phenyl-propyl ester

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