(2S,1'R)-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]-4-tert-butylcyclohexanone

Base Information

Chemical Name:(2S,1'R)-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]-4-tert-butylcyclohexanone
CAS No.:1187618-63-8
Molecular Formula:C₁₇H₂₃NO₄
Molecular Weight:305.374
Hs Code.:

Synonyms:(2S,1'R)-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]-4-tert-butylcyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,1'R)-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]-4-tert-butylcyclohexanone

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Technology Process of (2S,1'R)-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]-4-tert-butylcyclohexanone

There total 3 articles about (2S,1'R)-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]-4-tert-butylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 555-16-8
4-nitrobenzaldehdye

: 98-53-3
4-tercbutyl-cyclohexanone

: 1187618-63-8
(2S,1'R)-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]-4-tert-butylcyclohexanone

Guidance literature:: With 1,2-propylene cyclic carbonate; water; L-proline; at 20 ℃; for 24h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol1007313

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 98-53-3
4-tercbutyl-cyclohexanone

: 2-[1-hydroxy-1-(4-chlorophenyl)methyl]-4-tert-butylcyclohexan-1-one

: 1187618-63-8
(2S,1'R)-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]-4-tert-butylcyclohexanone

: C₁₇H₂₃NO₄

Guidance literature:: With [Cr₃O((S)-N-(pyridin-3-yl)-pyrrolidine-2-carboxamide)_1.8(H₂O)_0.2F(bdc)]*0.15(H₂bdc)*H₂O; In N,N-dimethyl-formamide; at 20 ℃; for 36h; optical yield given as %ee;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 98-53-3
4-tercbutyl-cyclohexanone

: 4-tert-butyl-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]cyclohexan-1-one

: 2-[1-hydroxy-1-(4-chlorophenyl)methyl]-4-tert-butylcyclohexan-1-one

: 1187618-63-8
(2S,1'R)-2-[1'-hydroxy-1'-(4-nitrophenyl)methyl]-4-tert-butylcyclohexanone

Guidance literature:: With L-Tryptophan; In 1,2-propylene cyclic carbonate; water; at 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1055/s-0030-1260038