(E)-1-(3-Benzyloxymethoxymethyl-cyclohex-1-enyl)-3-trimethylsilanyl-prop-2-en-1-ol

Base Information

Chemical Name:(E)-1-(3-Benzyloxymethoxymethyl-cyclohex-1-enyl)-3-trimethylsilanyl-prop-2-en-1-ol
CAS No.:108585-59-7
Molecular Formula:C₂₁H₃₂O₃Si
Molecular Weight:360.569
Hs Code.:

Synonyms:(E)-1-(3-Benzyloxymethoxymethyl-cyclohex-1-enyl)-3-trimethylsilanyl-prop-2-en-1-ol

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Chemical Property of (E)-1-(3-Benzyloxymethoxymethyl-cyclohex-1-enyl)-3-trimethylsilanyl-prop-2-en-1-ol

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Technology Process of (E)-1-(3-Benzyloxymethoxymethyl-cyclohex-1-enyl)-3-trimethylsilanyl-prop-2-en-1-ol

There total 1 articles about (E)-1-(3-Benzyloxymethoxymethyl-cyclohex-1-enyl)-3-trimethylsilanyl-prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 42201-74-1,78012-49-4
<β-(Trimethylsilyl)vinyl>magnesium bromide

: 97997-06-3
3-<(benzyloxy)methoxymethyl>-1-cyclohexenecarbaldehyde

: 108585-59-7
(E)-1-(3-Benzyloxymethoxymethyl-cyclohex-1-enyl)-3-trimethylsilanyl-prop-2-en-1-ol

Guidance literature:: In tetrahydrofuran; at -20 ℃;
DOI:10.1016/S0040-4020(01)90571-X

Reference yield: 91.0%

: 108585-59-7
(E)-1-(3-Benzyloxymethoxymethyl-cyclohex-1-enyl)-3-trimethylsilanyl-prop-2-en-1-ol

: 108585-63-3
E-1-(3'-benzyloxymethoxymethyl-1'-cyclohexenyl)-3-trimethylsilyl-2-propen-1-one

Guidance literature:: With nickel(IV) oxide; In diethyl ether; for 0.5h; Ambient temperature;
DOI:10.1016/S0040-4020(01)90571-X

Reference yield:

: 108585-59-7
(E)-1-(3-Benzyloxymethoxymethyl-cyclohex-1-enyl)-3-trimethylsilanyl-prop-2-en-1-ol

: 108585-85-9,108585-90-6
(3aR,4R,7aS)-4-Benzyloxymethoxymethyl-3a,4,5,6,7,7a-hexahydro-inden-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NiO₂ / diethyl ether / 0.5 h / Ambient temperature

2: FeCl₃ / CH₂Cl₂ / 2 h / 0 °C

With nickel(IV) oxide; iron(III) chloride; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)90571-X