C₈₀H₁₀₄O₃S₄Si₃

Base Information

• Chemical Name: C₈₀H₁₀₄O₃S₄Si₃
• CAS No.: 1185741-76-7
• Molecular Formula: C₈₀H₁₀₄O₃S₄Si₃
• Molecular Weight: 1326.22
• Mol file: 1185741-76-7.mol

Synonyms:C₈₀H₁₀₄O₃S₄Si₃

Chemical Property of C₈₀H₁₀₄O₃S₄Si₃

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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MSDS Files:

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Technology Process of C₈₀H₁₀₄O₃S₄Si₃

There total 1 articles about C₈₀H₁₀₄O₃S₄Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

Ph-4T-SnBu3 + C46H67IO3Si3 (1185741-75-6) → C80H104O3S4Si3 (1185741-76-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; Reflux;

DOI:10.1039/b906286f

Reference yield:

C80H104O3S4Si3 (1185741-76-7) → C62H62O3S4

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

DOI:10.1039/b906286f

Reference yield:

C80H104O3S4Si3 (1185741-76-7) → C62H59Br3S4 (1227007-64-8)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

2: carbon tetrabromide; triphenylphosphine / dichloromethane / 20 °C

With carbon tetrabromide; tetrabutyl ammonium fluoride; triphenylphosphine; In tetrahydrofuran; dichloromethane;

DOI:10.1039/b906286f

upstream raw materials:

C₄₆H₆₇IO₃Si₃

Downstream raw materials:

C₆₈H₆₈O₃S₄Se₃

C₆₂H₆₂S₄Se₃

C₆₅H₅₉N₃S₄Se₃

C₆₂H₅₉Br₃S₄