Acetic acid (S)-2-[(R)-2-(2-[1,3]dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethyl ester

Base Information

Chemical Name:Acetic acid (S)-2-[(R)-2-(2-[1,3]dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethyl ester
CAS No.:170710-88-0
Molecular Formula:C₂₁H₃₁NO₄
Molecular Weight:361.481
Hs Code.:

Synonyms:Acetic acid (S)-2-[(R)-2-(2-[1,3]dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethyl ester

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Chemical Property of Acetic acid (S)-2-[(R)-2-(2-[1,3]dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethyl ester

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Technology Process of Acetic acid (S)-2-[(R)-2-(2-[1,3]dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethyl ester

There total 6 articles about Acetic acid (S)-2-[(R)-2-(2-[1,3]dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: (S)-2-[2-(2-[1,3]Dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethanol

: 170710-88-0
Acetic acid (S)-2-[(R)-2-(2-[1,3]dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethyl ester

Guidance literature:: With dmap; In dichloromethane;
DOI:10.1021/jo00127a005

Reference yield:

: 1501-26-4
methyl 4-(chlorocarbonyl)butyrate

: 170710-88-0
Acetic acid (S)-2-[(R)-2-(2-[1,3]dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

2: KOH

4: Red-Al / tetrahydrofuran / Heating

5: 92 percent / DMAP / CH₂Cl₂

With dmap; potassium hydroxide; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00127a005

Reference yield:

: (1,3-dioxan-2-yl)ethylmagnesium bromide

: 170710-88-0
Acetic acid (S)-2-[(R)-2-(2-[1,3]dioxan-2-yl-ethyl)-piperidin-1-yl]-2-phenyl-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

2: KOH

4: Red-Al / tetrahydrofuran / Heating

5: 92 percent / DMAP / CH₂Cl₂

With dmap; potassium hydroxide; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00127a005