{Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2}⁽¹⁺⁾{Nb(3,5-dimethylphenoxide)6}^(1-)

Base Information

• Chemical Name: {Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2}⁽¹⁺⁾{Nb(3,5-dimethylphenoxide)6}^(1-)
• CAS No.: 101504-53-4
• Molecular Formula: C₂₈H₅₀NbO₂P₄*C₄₈H₅₄NbO₆
• Molecular Weight: 1455.36

Synonyms:{Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2}⁽¹⁺⁾{Nb(3,5-dimethylphenoxide)6}^(1-)

Chemical Property of {Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2}⁽¹⁺⁾{Nb(3,5-dimethylphenoxide)6}^(1-)

Chemical Property:

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Technology Process of {Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2}⁽¹⁺⁾{Nb(3,5-dimethylphenoxide)6}^(1-)

There total 2 articles about {Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2}⁽¹⁺⁾{Nb(3,5-dimethylphenoxide)6}^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2 (101461-80-7) + 3,5-Dimethylphenol (108-68-9,50356-23-5) → {Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2}(1+){Nb(3,5-dimethylphenoxide)6}(1-) (101504-53-4)

Guidance literature:

In benzene; byproducts: H2; to soln. of Nb complex was added neat 3,5-dimethylphenol with stirring, after 5 h crystals begun to form; crystals isolated after 15 h; elem. anal.;

DOI:10.1021/ja00195a030

Reference yield:

niobium di(3,5-dimethylphenoxide)di(bis(dimethylphosphino)ethane) (101461-80-7) + 3,5-Dimethylphenol (108-68-9,50356-23-5) → {Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2}(1+){Nb(3,5-dimethylphenoxide)6}(1-) (101504-53-4)

Guidance literature:

In neat (no solvent); byproducts: bis(dimethylphosphino)ethane, H2; rapidly;

upstream raw materials:

niobium di(3,5-dimethylphenoxide)di(bis(dimethylphosphino)ethane)

3,5-Dimethylphenol

Nb(3,5-dimethylphenoxide)2(1,2-bis(dimethylphosphino)ethane)2

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