methyl 3-acetoxy-3-[2-(carbomethoxymethyloxy)-5-methyl]phenyl-2-methylenepropanoate

Base Information

Chemical Name:methyl 3-acetoxy-3-[2-(carbomethoxymethyloxy)-5-methyl]phenyl-2-methylenepropanoate
CAS No.:1370710-83-0
Molecular Formula:C₁₇H₂₀O₇
Molecular Weight:336.342
Hs Code.:

Synonyms:methyl 3-acetoxy-3-[2-(carbomethoxymethyloxy)-5-methyl]phenyl-2-methylenepropanoate

Suppliers and Price of methyl 3-acetoxy-3-[2-(carbomethoxymethyloxy)-5-methyl]phenyl-2-methylenepropanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3-acetoxy-3-[2-(carbomethoxymethyloxy)-5-methyl]phenyl-2-methylenepropanoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3-acetoxy-3-[2-(carbomethoxymethyloxy)-5-methyl]phenyl-2-methylenepropanoate

There total 2 articles about methyl 3-acetoxy-3-[2-(carbomethoxymethyloxy)-5-methyl]phenyl-2-methylenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1370710-76-1
methyl 3-[2-(carbomethoxymethyloxy)-5-methyl]-phenyl-3-hydroxy-2-methylenepropanoate

: 108-24-7
acetic anhydride

: 1370710-83-0
methyl 3-acetoxy-3-[2-(carbomethoxymethyloxy)-5-methyl]phenyl-2-methylenepropanoate

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 1h;
DOI:10.5012/bkcs.2012.33.1.233

Reference yield:

: 24582-04-5
methyl (2-formyl-4-methylphenoxy)acetate

: 1370710-83-0
methyl 3-acetoxy-3-[2-(carbomethoxymethyloxy)-5-methyl]phenyl-2-methylenepropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-diaza-bicyclo[2.2.2]octane; triethanolamine / 288 h / 20 °C / Neat (no solvent)

2: dmap / dichloromethane / 1 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; dmap; triethanolamine; In dichloromethane; 1: Baylis-Hillman reaction;
DOI:10.5012/bkcs.2012.33.1.233