Cyclopropanecarboxylic acid, 2-(1E)-1-propenyl-, methyl ester, (1R,2S)- (9CI)

Base Information

Chemical Name:Cyclopropanecarboxylic acid, 2-(1E)-1-propenyl-, methyl ester, (1R,2S)- (9CI)
CAS No.:777918-01-1
Molecular Formula:C₈H₁₂O₂
Molecular Weight:140.182
Hs Code.:
Mol file:777918-01-1.mol

Synonyms:Cyclopropanecarboxylicacid, 2-(1E)-1-propenyl-, methyl ester, (1R,2S)- (9CI)

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Chemical Property of Cyclopropanecarboxylic acid, 2-(1E)-1-propenyl-, methyl ester, (1R,2S)- (9CI)

Chemical Property:

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Technology Process of Cyclopropanecarboxylic acid, 2-(1E)-1-propenyl-, methyl ester, (1R,2S)- (9CI)

There total 5 articles about Cyclopropanecarboxylic acid, 2-(1E)-1-propenyl-, methyl ester, (1R,2S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51974-60-8,112710-51-7
trans-1-hydroxymethyl-2(E)-propenylcyclopropane

: 176852-12-3,777918-01-1
methyl (-)-trans-2(E)-propenylcyclopropane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: CrO₃; aq. H₂SO₄ / acetone / 1 h

2: 0.3 g / diethyl ether / 0 °C

With chromium(VI) oxide; sulfuric acid; In diethyl ether; acetone;
DOI:10.1021/ja0305961

Reference yield:

: (-)-trans-1-cyano-2(E)-propenylcyclopropane

: 176852-12-3,777918-01-1
methyl (-)-trans-2(E)-propenylcyclopropane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / ethanol / 8 h / Heating

2: 0.3 g / diethyl ether / 0 °C

With sodium hydroxide; In diethyl ether; ethanol;
DOI:10.1021/ja0305961

Reference yield:

: (-)-trans-2(E)-propenylcyclopropane-1-carboxamide

: 176852-12-3,777918-01-1
methyl (-)-trans-2(E)-propenylcyclopropane-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 0.8 g / TsCl; pyridine / 8 h / 10 - 22 °C

2: aq. NaOH / ethanol / 8 h / Heating

3: 0.3 g / diethyl ether / 0 °C

With pyridine; sodium hydroxide; p-toluenesulfonyl chloride; In diethyl ether; ethanol;
DOI:10.1021/ja0305961