dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-β-L-glucopyranosyl) phosphate

Base Information

Chemical Name:dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-β-L-glucopyranosyl) phosphate
CAS No.:132867-82-4
Molecular Formula:C₃₄H₃₂IO₉P
Molecular Weight:742.501
Hs Code.:

Synonyms:dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-β-L-glucopyranosyl) phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-β-L-glucopyranosyl) phosphate

Chemical Property:

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Technology Process of dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-β-L-glucopyranosyl) phosphate

There total 5 articles about dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-β-L-glucopyranosyl) phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1623-08-1
phosphoric acid dibenzyl ester

: 132867-81-3
2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranosyl bromide

: 132867-82-4
dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-β-L-glucopyranosyl) phosphate

Guidance literature:: With silver carbonate; In diethyl ether; dichloromethane; acetonitrile;
DOI:10.1016/0008-6215(91)80150-L

Reference yield:

: 73-34-7,87-96-7,488-79-9,551-63-3,609-01-8,643-17-4,643-18-5,4164-09-4,6014-42-2,6155-36-8,6189-71-5,6696-41-9,6736-43-2,13224-93-6,22611-09-2,28161-49-1,28161-50-4,28161-52-6,45864-36-6,63814-64-2,71116-59-1,71116-61-5,72598-05-1,87936-88-7,87936-89-8,97466-79-0,116908-82-8,120442-60-6,123484-22-0,133576-32-6
6-deoxy-L-galactose

: 132867-82-4
dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-β-L-glucopyranosyl) phosphate

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / pyridine / 0.2 h / -40 °C

2: sodium iodide / dimethylformamide / Ambient temperature

3: 91 percent / 30percent hydrogen bromide / CH₂Cl₂; acetic acid / 5 h / Ambient temperature

4: 91 percent / silver carbonate / CH₂Cl₂; diethyl ether; acetonitrile

With pyridine; hydrogen bromide; silver carbonate; sodium iodide; In diethyl ether; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(91)80150-L

Reference yield:

: 132867-78-8
1,2,3-tri-O-benzoyl-4,6-dideoxy-4-iodo-α-L-glucopyranose

: 132867-82-4
dibenzyl (2,3-di-O-benzoyl-4,6-dideoxy-4-iodo-β-L-glucopyranosyl) phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / 30percent hydrogen bromide / CH₂Cl₂; acetic acid / 5 h / Ambient temperature

2: 91 percent / silver carbonate / CH₂Cl₂; diethyl ether; acetonitrile

With hydrogen bromide; silver carbonate; In diethyl ether; dichloromethane; acetic acid; acetonitrile;
DOI:10.1016/0008-6215(91)80150-L