Technology Process of C28H34N12O6
There total 6 articles about C28H34N12O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 96 percent / NaH; TBAI / dimethylformamide / 2 h / 20 °C
2: aq. acetic acid / dioxane / 10 h / 75 - 80 °C
With
tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid;
In
1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1021/ja048936l
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 92 percent / imidazole / dimethylformamide / 24 h / 20 °C
2: 93 percent / sodium methoxide / methanol / 5 h / 20 °C
3: 95 percent / p-toluenesulfonic acid / 10 h / 20 °C
4: 100 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C
5: 96 percent / NaH; TBAI / dimethylformamide / 2 h / 20 °C
6: aq. acetic acid / dioxane / 10 h / 75 - 80 °C
With
1H-imidazole; tetrabutyl ammonium fluoride; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; acetic acid;
In
tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja048936l
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 93 percent / sodium methoxide / methanol / 5 h / 20 °C
2: 95 percent / p-toluenesulfonic acid / 10 h / 20 °C
3: 100 percent / tetrabutylammonium fluoride / tetrahydrofuran / 1 h / 20 °C
4: 96 percent / NaH; TBAI / dimethylformamide / 2 h / 20 °C
5: aq. acetic acid / dioxane / 10 h / 75 - 80 °C
With
tetrabutyl ammonium fluoride; sodium methylate; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; acetic acid;
In
tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja048936l