C₆₅H₈₀N₆O₂₇

Base Information

• Chemical Name: C₆₅H₈₀N₆O₂₇
• CAS No.: 444118-85-8
• Molecular Formula: C₆₅H₈₀N₆O₂₇
• Molecular Weight: 1377.37
• Mol file: 444118-85-8.mol

Synonyms:C₆₅H₈₀N₆O₂₇

Chemical Property of C₆₅H₈₀N₆O₂₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₅H₈₀N₆O₂₇

There total 1 articles about C₆₅H₈₀N₆O₂₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

C71H94N6O27Si → C65H80N6O27 (444118-85-8)

Guidance literature:

With pyridine hydrogenfluoride; acetic acid; In tetrahydrofuran; at 20 ℃; for 72h;

DOI:10.1002/chem.200390009

Reference yield: 90.0%

C65H80N6O27 (444118-85-8) → pent-4-enyl (3,6-di-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-(6-O-acetyl-3-O-benzyl-2-azido-2-deoxy-α-D-glucopyranosyl)-(1->4)-(methyl 3-O-benzyl-β-D-glucopyranosyluronate

Guidance literature:

With pyridine; thiourea; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1002/chem.200390009

Reference yield:

C65H80N6O27 (444118-85-8) → pent-4-enyl (3,6-di-O-acetyl-2-azido-2-deoxy-α-D-glucopyranosyl)-(1->4)-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-(1->4)-(6-O-acetyl-3-O-benzyl-2-azido-2-deoxy-α-D-glucopyranosyl)-(1->4)-(methyl 2,3-di-O-benzyl-β-D-glucopyranosyluronate

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / thiourea; pyridine / dimethylformamide / 24 h / 20 °C

2: 76 percent / molecular sieves 4 Angstroem; Ag₂O / CH₂Cl₂ / 20 °C

With pyridine; 4 A molecular sieve; thiourea; silver(l) oxide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1002/chem.200390009