acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester

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Chemical Name:acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester
CAS No.:239466-02-5
Molecular Formula:C₄₄H₅₇NO₂₄S
Molecular Weight:1015.99
Hs Code.:

acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester

Synonyms:acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester

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Chemical Property of acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester

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Technology Process of acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester

There total 1 articles about acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 108-24-7
acetic anhydride

: 239466-01-4
N-[2-(4,5-dihydroxy-6-hydroxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yloxy)-4-hydroxy-6-hydroxymethyl-5-(3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

: 239466-02-5
acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester

Guidance literature:: With pyridine;
DOI:10.1016/S0040-4039(99)00930-2

Reference yield: 98.0%

: C₁₉H₁₉NO₆

: 239466-02-5
acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester

: C₅₇H₇₀N₂O₃₀

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In dichloromethane; at -78 ℃;
DOI:10.1016/S0040-4039(99)00930-2

Reference yield:

: 239466-02-5
acetic acid 3-acetoxy-5-[4-acetoxy-6-acetoxymethyl-3-acetylamino-5-(3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-2-acetoxymethyl-6-phenylsulfanyl-tetrahydro-pyran-4-yl ester

: 239466-05-8
3-{3-[3-acetylamino-4-hydroxy-6-hydroxymethyl-5-(3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy}-2-benzyloxycarbonylamino-propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / NIS; TfOH / CH₂Cl₂ / -78 °C

2: Zn; AcOH; H₂O / 20 °C

3: NaOMe / methanol / 0 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; water; sodium methylate; acetic acid; zinc; In methanol; dichloromethane; 1: Etherification / 2: Reduction / 3: Deacetylation;
DOI:10.1016/S0040-4039(99)00930-2