(2S,3S)-2-tert-Butoxycarbonylamino-3-formyl-5-phenyl-pentanoic acid methyl ester

Base Information

• Chemical Name: (2S,3S)-2-tert-Butoxycarbonylamino-3-formyl-5-phenyl-pentanoic acid methyl ester
• CAS No.: 749927-05-7
• Molecular Formula: C₁₈H₂₅NO₅
• Molecular Weight: 335.4

Synonyms:(2S,3S)-2-tert-Butoxycarbonylamino-3-formyl-5-phenyl-pentanoic acid methyl ester

Chemical Property of (2S,3S)-2-tert-Butoxycarbonylamino-3-formyl-5-phenyl-pentanoic acid methyl ester

Chemical Property:

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Technology Process of (2S,3S)-2-tert-Butoxycarbonylamino-3-formyl-5-phenyl-pentanoic acid methyl ester

There total 1 articles about (2S,3S)-2-tert-Butoxycarbonylamino-3-formyl-5-phenyl-pentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(2S,3R)-2-tert-Butoxycarbonylamino-3-phenethyl-pent-4-enoic acid methyl ester (749927-03-5) → (2S,3S)-2-tert-Butoxycarbonylamino-3-formyl-5-phenyl-pentanoic acid methyl ester (749927-05-7) + (2S,3S)-2-tert-Butoxycarbonylamino-3-phenethyl-succinic acid 1-methyl ester

Guidance literature:

With sodium periodate; osmium(VIII) oxide; In water; acetone; at 0 - 20 ℃; for 24h; Title compound not separated from byproducts.;

DOI:10.1016/j.tetlet.2004.05.157

Reference yield: 100.0%

(2S,3S)-2-tert-Butoxycarbonylamino-3-formyl-5-phenyl-pentanoic acid methyl ester (749927-05-7) → (2S,3S)-2-tert-Butoxycarbonylamino-3-phenethyl-succinic acid 1-methyl ester

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In acetone;

DOI:10.1016/j.tetlet.2004.05.157

Reference yield: 45.0%

(2S,3S)-2-tert-Butoxycarbonylamino-3-formyl-5-phenyl-pentanoic acid methyl ester (749927-05-7) → ((3S,4S)-2-Oxo-4-phenethyl-tetrahydro-furan-3-yl)-carbamic acid tert-butyl ester

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 0.5h;

DOI:10.1016/j.tetlet.2004.05.157

upstream raw materials:

(2S,3R)-2-tert-Butoxycarbonylamino-3-phenethyl-pent-4-enoic acid methyl ester

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