Technology Process of C17H22O5
There total 9 articles about C17H22O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
for 1.5h;
Inert atmosphere;
DOI:10.1021/ol500788c
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium triethylborohydride / tetrahydrofuran / 6.25 h / 20 - 45 °C / Inert atmosphere
2: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / 0 - 20 °C / Inert atmosphere
3: 4-methyl-morpholine / dichloromethane / 2 h / 20 °C / Inert atmosphere
4: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 24 h / 20 °C
5: samarium diiodide / acetonitrile; methanol / 1 h / -20 °C / Inert atmosphere
6: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
With
4-methyl-morpholine; samarium diiodide; boron trifluoride diethyl etherate; lithium triethylborohydride; sodium hydrogencarbonate; Dess-Martin periodane; methyl iodide;
In
tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
6: |Dess-Martin Oxidation;
DOI:10.1021/ol500788c
- Guidance literature:
-
Multi-step reaction with 5 steps
1: boron trifluoride diethyl etherate / dichloromethane / 0.67 h / 0 - 20 °C / Inert atmosphere
2: 4-methyl-morpholine / dichloromethane / 2 h / 20 °C / Inert atmosphere
3: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 24 h / 20 °C
4: samarium diiodide / acetonitrile; methanol / 1 h / -20 °C / Inert atmosphere
5: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere
With
4-methyl-morpholine; samarium diiodide; boron trifluoride diethyl etherate; sodium hydrogencarbonate; Dess-Martin periodane; methyl iodide;
In
methanol; dichloromethane; water; acetonitrile;
5: |Dess-Martin Oxidation;
DOI:10.1021/ol500788c