allyl 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside

Base Information

• Chemical Name: allyl 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside
• CAS No.: 946495-23-4
• Molecular Formula: C₂₅H₂₆FNO₇
• Molecular Weight: 471.482
• Mol file: 946495-23-4.mol

Synonyms:allyl 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside

Chemical Property of allyl 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of allyl 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside

There total 1 articles about allyl 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

Allyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosid (141019-98-9) → allyl 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside (946495-23-4)

Guidance literature:

With diethylamino-sulfur trifluoride; In dichloromethane; at -42 - 20 ℃; for 16.0833h;

Reference yield: 79.0%

allyl 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside (946495-23-4) → 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-gIucopyranose (946495-28-9)

Guidance literature:

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In acetic acid; at 80 ℃; for 2h;

Reference yield: 79.0%

allyl 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside (946495-23-4) → 2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-D-glucopyranose

Guidance literature:

With acetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; at 80 ℃; for 2h;

DOI:10.1016/j.tetasy.2007.05.032

upstream raw materials:

Allyl-2-acetamido-3,6-di-O-benzoyl-2-desoxy-α-D-galactopyranosid

Downstream raw materials:

dibenzylphosphate-2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-glucopyranoside

2-acetamido-3,6-di-O-benzoyl-2,4-dideoxy-4-fluoro-α-D-gIucopyranose