10-eicosenyl-1,20-ditosylate

Base Information

• Chemical Name: 10-eicosenyl-1,20-ditosylate
• CAS No.: 83932-93-8
• Molecular Formula: C₃₄H₅₂O₆S₂
• Molecular Weight: 620.915
• Mol file: 83932-93-8.mol

Synonyms:10-eicosenyl-1,20-ditosylate

Chemical Property of 10-eicosenyl-1,20-ditosylate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 10-eicosenyl-1,20-ditosylate

There total 1 articles about 10-eicosenyl-1,20-ditosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

10-undecen-1-yl p-toluenesulfonate (51148-67-5) → 10-eicosenyl-1,20-ditosylate (83932-93-8) + 10-eicosenyl-1,20-ditosylate (83932-88-1)

Guidance literature:

trimethyltin(IV)chloride; tungsten(VI) chloride; In chlorobenzene; at 60 ℃; for 24h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1016/S0040-4039(00)87516-4

Reference yield: 98.0%

10-eicosenyl-1,20-ditosylate (83932-93-8) → icosane-1,20-diyl bis(4-methylbenzenesulfonate) (83932-91-6)

Guidance literature:

With hydrogen; palladium;

DOI:10.1016/S0040-4039(00)87516-4

Reference yield:

10-eicosenyl-1,20-ditosylate (83932-93-8) → docosanedinitrile (5634-23-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / H₂ / palladium

2: dimethylsulfoxide

With hydrogen; palladium; In dimethyl sulfoxide;

DOI:10.1016/S0040-4039(00)87516-4

upstream raw materials:

10-undecen-1-yl p-toluenesulfonate

Downstream raw materials:

10-hydroxydecyl 4-methylbenzenesulfonate

icosane-1,20-diyl bis(4-methylbenzenesulfonate)

docosanedinitrile