6-nitro-2-phenylsulphonylbenzothiazole

Base Information

• Chemical Name: 6-nitro-2-phenylsulphonylbenzothiazole
• CAS No.: 76007-15-3
• Molecular Formula: C₁₃H₈N₂O₄S₂
• Molecular Weight: 320.35
• Mol file: 76007-15-3.mol

Synonyms:6-nitro-2-phenylsulphonylbenzothiazole

Chemical Property of 6-nitro-2-phenylsulphonylbenzothiazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-nitro-2-phenylsulphonylbenzothiazole

There total 2 articles about 6-nitro-2-phenylsulphonylbenzothiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

6-nitro-2-phenylsulfanylbenzothiazole (38420-80-3) → 6-nitro-2-phenylsulphonylbenzothiazole (76007-15-3)

Guidance literature:

With sulfuric acid; dihydrogen peroxide; In acetic acid; at 80 ℃; for 1h;

DOI:10.1039/P19800002362

Reference yield: 64.0%

2-chloro-6-nitrobenzothiazole (2407-11-6) + sodium benzenesulfonate (873-55-2) → 6-nitro-2-phenylsulphonylbenzothiazole (76007-15-3)

Guidance literature:

With acetic acid; In water; at 90 ℃; for 2h;

DOI:10.1002/chem.202102124

Reference yield: 52.0%

6-nitro-2-phenylsulphonylbenzothiazole (76007-15-3) → 6-amino-2-phenylsulphonylbenzothiazole (76006-92-3)

Guidance literature:

With iron; acetic acid; In ethanol; water; Heating;

DOI:10.1039/P19800002362

upstream raw materials:

2-chloro-6-nitrobenzothiazole

sodium benzenesulfonate

6-nitro-2-phenylsulfanylbenzothiazole

Downstream raw materials:

6-amino-2-phenylsulphonylbenzothiazole