(E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid

Base Information

Chemical Name:(E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid
CAS No.:129813-32-7
Molecular Formula:C₁₈H₁₇NO₄
Molecular Weight:311.337
Hs Code.:

Synonyms:(E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid

Suppliers and Price of (E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Pictogram(s):
Hazard Codes:

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Useful:

Technology Process of (E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid

There total 2 articles about (E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: (E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid ethyl ester

: 129813-32-7
(E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid

Guidance literature:: With hydrogenchloride; for 2h; Heating;
DOI:10.1021/jm00105a042

Reference yield:

: 129813-55-4
ethyl 3-<4-(3-pyridylmethyl)-2,5-dimethoxy-3,6-dimethylphenyl>-2-methylacrylate

: 129813-32-7
(E)-3-(2,5-Dimethyl-3,6-dioxo-4-pyridin-3-ylmethyl-cyclohexa-1,4-dienyl)-2-methyl-acrylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: cerium ammonium nitrate (CAN) / H₂O; acetonitrile / 1 h / 0 °C

2: 70 percent / concd. aq. HCl / 2 h / Heating

With hydrogenchloride; ammonium cerium(IV) nitrate; In water; acetonitrile;
DOI:10.1021/jm00105a042