1,6,9-tris(4-tert-butylphenoxy)-N-(4-ethynylphenyl)perylene-3,4-dicarboximide

Base Information

• Chemical Name: 1,6,9-tris(4-tert-butylphenoxy)-N-(4-ethynylphenyl)perylene-3,4-dicarboximide
• CAS No.: 524960-80-3
• Molecular Formula: C₆₀H₅₁NO₅
• Molecular Weight: 866.069
• Mol file: 524960-80-3.mol

Synonyms:1,6,9-tris(4-tert-butylphenoxy)-N-(4-ethynylphenyl)perylene-3,4-dicarboximide

Chemical Property of 1,6,9-tris(4-tert-butylphenoxy)-N-(4-ethynylphenyl)perylene-3,4-dicarboximide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,6,9-tris(4-tert-butylphenoxy)-N-(4-ethynylphenyl)perylene-3,4-dicarboximide

There total 1 articles about 1,6,9-tris(4-tert-butylphenoxy)-N-(4-ethynylphenyl)perylene-3,4-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

4-Ethynylaniline (14235-81-5) + 1,6,9-tris(4-tert-butylphenoxy)perylene-3,4-dicarboxylic anhydride (524960-75-6) → 1,6,9-tris(4-tert-butylphenoxy)-N-(4-ethynylphenyl)perylene-3,4-dicarboximide (524960-80-3)

Guidance literature:

With zinc diacetate; In N,N-dimethyl-formamide; at 130 ℃; for 17h;

DOI:10.1016/S0040-4020(03)00020-6

Reference yield: 69.0%

3,5-dibromobenzaldehyde (56990-02-4) + 1,6,9-tris(4-tert-butylphenoxy)-N-(4-ethynylphenyl)perylene-3,4-dicarboximide (524960-80-3) → 3,5-bis[2-[4-[1,6,9-tris(4-tert-butylphenoxy)perylene-3,4-dicarboximido]phenyl]ethynyl]benzaldehyde

Guidance literature:

With copper(l) iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; triphenylphosphine; In toluene; at 50 ℃; for 23h;

DOI:10.1016/S0040-4020(03)00020-6

Reference yield:

1,6,9-tris(4-tert-butylphenoxy)-N-(4-ethynylphenyl)perylene-3,4-dicarboximide (524960-80-3) → C52H46O7(2-)*2K(1+)

Guidance literature:

With potassium hydroxide; In tert-butyl alcohol; for 2h; Heating;

DOI:10.1016/S0040-4020(03)00020-6

upstream raw materials:

4-Ethynylaniline

1,6,9-tris(4-tert-butylphenoxy)perylene-3,4-dicarboxylic anhydride