(Z,Z)-2,2'-thiobis(3-(4-chlorophenyl)-1-phenylprop-2-en-1-one)

Base Information

• Chemical Name: (Z,Z)-2,2'-thiobis(3-(4-chlorophenyl)-1-phenylprop-2-en-1-one)
• CAS No.: 242133-10-4
• Molecular Formula: C₃₀H₂₀Cl₂O₂S
• Molecular Weight: 515.46
• Mol file: 242133-10-4.mol

Synonyms:(Z,Z)-2,2'-thiobis(3-(4-chlorophenyl)-1-phenylprop-2-en-1-one)

Chemical Property of (Z,Z)-2,2'-thiobis(3-(4-chlorophenyl)-1-phenylprop-2-en-1-one)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (Z,Z)-2,2'-thiobis(3-(4-chlorophenyl)-1-phenylprop-2-en-1-one)

There total 2 articles about (Z,Z)-2,2'-thiobis(3-(4-chlorophenyl)-1-phenylprop-2-en-1-one) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

diphenacyl sulfide (2461-80-5) + 4-chlorobenzaldehyde (104-88-1) → 2-[(5Z)-5-(p-chlorobenzylidene)-2-(p-chlorophenyl)-2,5-dihydro-4-phenylthiazol-2-yl]-1-phenylethanone + (Z,Z)-2,2'-thiobis(3-(4-chlorophenyl)-1-phenylprop-2-en-1-one) (242133-10-4)

Guidance literature:

With ammonium acetate; for 0.166667h; microwave irradiation;

DOI:10.1016/j.tet.2007.07.040

Reference yield:

diphenacyl sulfide (2461-80-5) + 4-chlorobenzaldehyde (104-88-1) → (Z,Z)-2,2'-thiobis(3-(4-chlorophenyl)-1-phenylprop-2-en-1-one) (242133-10-4)

Guidance literature:

DOI:10.1023/A:1013795006690

Reference yield: 83.0%

nitromethane (75-52-5) + (Z,Z)-2,2'-thiobis(3-(4-chlorophenyl)-1-phenylprop-2-en-1-one) (242133-10-4) → 2a,6e-dibenzoyl-3a,5e-di(p-chlorophenyl)-4e-nitrothiane

Guidance literature:

With sodium ethanolate; In ethanol; at 110 ℃; for 0.133333h; Solvent; stereoselective reaction; Sealed tube; Microwave irradiation;

DOI:10.1080/00397911.2012.683970

upstream raw materials:

diphenacyl sulfide

4-chlorobenzaldehyde

Downstream raw materials:

3-(4-chlorophenyl)-1-phenylprop-2-en-1-one

2e,6e-dibenzoyl-3e,5e-di(p-chlorophenyl)-4e-nitrothiane

trans-(4,4'-thiobis(3-(4-chlorophenyl)-5-phenyl-2,3-dihydrofuran-4,2-diyl))bis(phenylmethanone)

trans-(4,4'-thiobis(3-(4-chlorophenyl)-5-phenyl-2,3-dihydrofuran-4,2-diyl))bis((4-chlorophenyl)methanone)