Technology Process of C29H24F6N2O4
There total 7 articles about C29H24F6N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine;
In
dichloromethane;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 0.75 h / 130 °C
2.1: acetyl chloride / 1 h / 64 °C
3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -50 °C
3.2: 1 h / -50 - 20 °C
4.1: water; lithium hydroxide / methanol / 1 h / 20 - 75 °C / a sealed vial
5.1: pyridine / 0.75 h
5.2: pH 4
6.1: triethylamine; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / dichloromethane / 4 h / 20 °C
With
pyridine; water; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine; acetyl chloride; lithium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 0.75 h / 130 °C
2.1: acetyl chloride / 1 h / 64 °C
3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -50 °C
3.2: 1 h / -50 - 20 °C
4.1: water; lithium hydroxide / methanol / 1 h / 20 - 75 °C / a sealed vial
5.1: pyridine / 0.75 h
5.2: pH 4
6.1: triethylamine; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / dichloromethane / 4 h / 20 °C
With
pyridine; water; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine; acetyl chloride; lithium hydroxide; lithium hexamethyldisilazane;
In
tetrahydrofuran; methanol; dichloromethane;
