1-(2-methoxyphenyl)-4-amino-6-methoxy-2,3-dihydropyrrolo<3,2-c>quinoline

Base Information

Chemical Name:1-(2-methoxyphenyl)-4-amino-6-methoxy-2,3-dihydropyrrolo<3,2-c>quinoline
CAS No.:122456-35-3
Molecular Formula:C₁₉H₁₉N₃O₂
Molecular Weight:321.379
Hs Code.:

Synonyms:1-(2-methoxyphenyl)-4-amino-6-methoxy-2,3-dihydropyrrolo<3,2-c>quinoline

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Chemical Property of 1-(2-methoxyphenyl)-4-amino-6-methoxy-2,3-dihydropyrrolo<3,2-c>quinoline

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Technology Process of 1-(2-methoxyphenyl)-4-amino-6-methoxy-2,3-dihydropyrrolo<3,2-c>quinoline

There total 3 articles about 1-(2-methoxyphenyl)-4-amino-6-methoxy-2,3-dihydropyrrolo<3,2-c>quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanolic ammonia: methanolic ammonia

: 122456-32-0
1-(2-methoxyphenyl)-4-oxo-6-methoxy-2,3,4,5-tetrahydropyrrolo<3,2-c>quinoline

: 7450-69-3
phenyl diamidophosphate

: 122456-35-3
1-(2-methoxyphenyl)-4-amino-6-methoxy-2,3-dihydropyrrolo<3,2-c>quinoline

Guidance literature:: With sodium hydroxide; In dichloromethane;

Reference yield:

: 122456-55-7
2-(2-ethoxyethyl)-N,N'-bis(2-methoxyphenyl)malondiamide

: 122456-35-3
1-(2-methoxyphenyl)-4-amino-6-methoxy-2,3-dihydropyrrolo<3,2-c>quinoline

Guidance literature:: With phenyl diamidophosphate; Yield given. Multistep reaction; 1.) diphenyl ether, reflux, 9 h, 2.) a) 230 deg C, 45 min, b) diphenyl ether, 230 deg C, 15 min;
DOI:10.1021/jm00088a021

Reference yield:

: 13487-89-3
diethyl 2-ethoxyethylmalonate

: 122456-35-3
1-(2-methoxyphenyl)-4-amino-6-methoxy-2,3-dihydropyrrolo<3,2-c>quinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 36.6 g / 3 h / 200 °C

2: 2.) phenyl phosphorodiamidate / 1.) diphenyl ether, reflux, 9 h, 2.) a) 230 deg C, 45 min, b) diphenyl ether, 230 deg C, 15 min

With phenyl diamidophosphate;
DOI:10.1021/jm00088a021