C₂₀H₃₂O₆

Base Information

Chemical Name:C₂₀H₃₂O₆
CAS No.:952492-27-2
Molecular Formula:C₂₀H₃₂O₆
Molecular Weight:368.47
Hs Code.:

C<sub>20</sub>H<sub>32</sub>O<sub>6</sub>

Synonyms:C₂₀H₃₂O₆

Suppliers and Price of C₂₀H₃₂O₆

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₀H₃₂O₆

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₀H₃₂O₆

There total 19 articles about C₂₀H₃₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 952492-26-1
C₁₉H₂₈O₆

: 952492-27-2
C₂₀H₃₂O₆

Guidance literature:: C₁₉H₂₈O₆; Me₂CuLi; In diethyl ether; at -20 - 20 ℃;

With sodium periodate; In tetrahydrofuran; water; at 0 - 20 ℃; for 3h; Further stages.;
DOI:10.1016/j.tetlet.2007.07.068

Reference yield:

: 952492-20-5
C₂₆H₄₄O₄Si

: 952492-27-2
C₂₀H₃₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: 91 percent / OsO₄; NMO / acetone; H₂O / 72 h / 20 °C

2.1: 2,6-lutidine / CH₂Cl₂ / 0.08 h / 0 °C

3.1: DIBAL-H / CH₂Cl₂ / 0.33 h / -78 °C

4.1: MsCl; Et₃N; DMAP / CH₂Cl₂ / 0.25 h / 0 °C

4.2: 52 percent / K₂CO₃ / methanol / 18 h / 20 °C

5.1: CSA / CH₂Cl₂; methanol / 6 h / 0 °C

6.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2 h / -78 °C

7.1: CH₂Cl₂ / 72 h / 20 °C

8.1: DIBAL-H / CH₂Cl₂ / 0.25 h / -78 °C

9.1: TBAF / tetrahydrofuran / 6 h / 0 - 20 °C

10.1: Ti(OiPr)4; (+)-DIPT; TBHP / 4A MS / CH₂Cl₂ / 8 h / -20 °C

11.1: diethyl ether / -20 - 20 °C

11.2: 55 percent / NaIO₄ / tetrahydrofuran; H₂O / 3 h / 0 - 20 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; osmium(VIII) oxide; N-methyl-2-indolinone; oxalyl dichloride; L-(+)-diisopropyl tartrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; dimethyl sulfoxide; methanesulfonyl chloride; triethylamine; 4A MS; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; 10.1: Katsuki-Sharpless epoxidation;
DOI:10.1016/j.tetlet.2007.07.068

Reference yield:

: C₂₆H₄₆O₅Si

: 952492-27-2
C₂₀H₃₂O₆

Guidance literature:: Multi-step reaction with 6 steps

1.1: (COCl)2; DMSO; Et₃N / CH₂Cl₂ / 2 h / -78 °C

2.1: CH₂Cl₂ / 72 h / 20 °C

3.1: DIBAL-H / CH₂Cl₂ / 0.25 h / -78 °C

4.1: TBAF / tetrahydrofuran / 6 h / 0 - 20 °C

5.1: Ti(OiPr)4; (+)-DIPT; TBHP / 4A MS / CH₂Cl₂ / 8 h / -20 °C

6.1: diethyl ether / -20 - 20 °C

6.2: 55 percent / NaIO₄ / tetrahydrofuran; H₂O / 3 h / 0 - 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; oxalyl dichloride; L-(+)-diisopropyl tartrate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; 4A MS; In tetrahydrofuran; diethyl ether; dichloromethane; 5.1: Katsuki-Sharpless epoxidation;
DOI:10.1016/j.tetlet.2007.07.068