Cyclohex-3-enecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester

Base Information

• Chemical Name: Cyclohex-3-enecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester
• CAS No.: 197148-64-4
• Molecular Formula: C₁₂H₁₃NO₂S
• Molecular Weight: 235.307
• Mol file: 197148-64-4.mol

Synonyms:Cyclohex-3-enecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester

Chemical Property of Cyclohex-3-enecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester

Chemical Property:

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Technology Process of Cyclohex-3-enecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester

There total 1 articles about Cyclohex-3-enecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-hydroxy-2(1H)-pyridinethione (1121-30-8) + 1,2,5,6-tetrahydrobenzoic acid (4771-80-6) → Cyclohex-3-enecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester (197148-64-4)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; Yield given; Ambient temperature;

DOI:10.1021/jo970639u

Reference yield: 68.0%

Cyclohex-3-enecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester (197148-64-4) → 4-(2-pyridylthio)cyclohexene + 4-[2,2-dichloro-1,1-difluoro-2-(2-pyridylthio)ethyl]cyclohexene

Guidance literature:

With 1,1'-dichloro-2,2'-difluoroethene; In dichloromethane; for 5h; Irradiation;

DOI:10.1021/jo970639u

Reference yield: 13.0%

1,1'-dichloro-2,2'-difluoroethene (79-35-6) + Cyclohex-3-enecarboxylic acid 2-thioxo-2H-pyridin-1-yl ester (197148-64-4) → 4-(2-pyridylthio)cyclohexene + 4-[2,2-dichloro-1,1-difluoro-2-(2-pyridylthio)ethyl]cyclohexene

Guidance literature:

In dichloromethane; for 5h; Irradiation;

DOI:10.1021/jo970639u

upstream raw materials:

1-hydroxy-2(1H)-pyridinethione

1,2,5,6-tetrahydrobenzoic acid