L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R,2R),6aα>>-

Base Information

Chemical Name:L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R*,2R*),6aα>>-
CAS No.:153805-39-1
Molecular Formula:C₂₇H₄₈N₄O₄S
Molecular Weight:524.769
Hs Code.:

L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R*,2R*),6aα>>-

Synonyms:L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R*,2R*),6aα>>-

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Chemical Property of L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R*,2R*),6aα>>-

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Technology Process of L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R*,2R*),6aα>>-

There total 6 articles about L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R*,2R*),6aα>>- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 153805-38-0
carbamic acid, <1-<2,2-dimethyl-5-<2-cyclohexyl-1-<<<2-methyl-1-<<(2-pyridinylmethyl)amino>carbonyl>butyl>amino>carbonyl>ethyl>-1,3-dioxolan-4-yl>-2-methylpropyl>-, 1,1-dimethylethyl ester, <4R-<4α(R*),5β(S*)>>

: 153805-39-1
L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R*,2R*),6aα>>-

Guidance literature:: With methanol; ethandithiol; acetyl chloride; for 6h; Ambient temperature;
DOI:10.1021/jm00028a013

Reference yield:

: 137-00-8,8042-97-5
5-hydroxyethyl-4-methylthiazole

: 153805-39-1
L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R*,2R*),6aα>>-

Guidance literature:: Multi-step reaction with 6 steps

1: 54 percent / ZnN₆-pyridine2, PPh₃, diisopropyl azodicarboxylate / toluene / 3 h / Ambient temperature

2: 97 percent / H₂ / Pd/CaCO₃ / methanol / 2.5 h / 760 Torr

3: 97 percent / iPr₂EtN, (EtO)2P(O)CN / CH₂Cl₂ / 20 h / Ambient temperature

4: 91 percent / CF₃CO₂H / CH₂Cl₂ / 1 h / Ambient temperature

5: 80 percent / iPr₂EtN, (EtO)2P(O)CN / CH₂Cl₂ / 14 h / Ambient temperature

6: 75 percent / acetyl chloride, methanol, ethanedithiol / 6 h / Ambient temperature

With methanol; ethandithiol; diethyl cyanophosphonate; di-isopropyl azodicarboxylate; ZnN₆-pyridine2; hydrogen; N-ethyl-N,N-diisopropylamine; acetyl chloride; triphenylphosphine; trifluoroacetic acid; Lindlar's catalyst; In methanol; dichloromethane; toluene;
DOI:10.1021/jm00028a013

Reference yield:

: 153805-36-8
5-(2-azidoethyl)-4-methylthiazole

: 153805-39-1
L-idonamide, 6-cyclohexyl-2,5,6-trideoxy-5-amino-2-(1-methylethyl)-N-<2-methyl-1-<<<2-(4-methyl-5-thiazolyl)ethyl>amino>carbonyl>butyl>-, <3aS-<3aα,4β(1R*,2R*),6aα>>-

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / H₂ / Pd/CaCO₃ / methanol / 2.5 h / 760 Torr

2: 97 percent / iPr₂EtN, (EtO)2P(O)CN / CH₂Cl₂ / 20 h / Ambient temperature

3: 91 percent / CF₃CO₂H / CH₂Cl₂ / 1 h / Ambient temperature

4: 80 percent / iPr₂EtN, (EtO)2P(O)CN / CH₂Cl₂ / 14 h / Ambient temperature

5: 75 percent / acetyl chloride, methanol, ethanedithiol / 6 h / Ambient temperature

With methanol; ethandithiol; diethyl cyanophosphonate; hydrogen; N-ethyl-N,N-diisopropylamine; acetyl chloride; trifluoroacetic acid; Lindlar's catalyst; In methanol; dichloromethane;
DOI:10.1021/jm00028a013