(R)-N-[1-(1,3-Benzodioxol-5-yl)butylidene]-α-methylbenzene-methanamine

Base Information

• Chemical Name: (R)-N-[1-(1,3-Benzodioxol-5-yl)butylidene]-α-methylbenzene-methanamine
• CAS No.: 197508-43-3
• Molecular Formula: C₁₉H₂₁NO₂
• Molecular Weight: 295.381

Synonyms:(R)-N-[1-(1,3-Benzodioxol-5-yl)butylidene]-α-methylbenzene-methanamine

Chemical Property of (R)-N-[1-(1,3-Benzodioxol-5-yl)butylidene]-α-methylbenzene-methanamine

Chemical Property:

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Technology Process of (R)-N-[1-(1,3-Benzodioxol-5-yl)butylidene]-α-methylbenzene-methanamine

There total 1 articles about (R)-N-[1-(1,3-Benzodioxol-5-yl)butylidene]-α-methylbenzene-methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

→ (R)-N-[1-(1,3-Benzodioxol-5-yl)butylidene]-α-methylbenzene-methanamine (197508-43-3)

Guidance literature:

Reference yield:

(R)-N-[1-(1,3-Benzodioxol-5-yl)butylidene]-α-methylbenzene-methanamine (197508-43-3) → C19H23NO2 + C19H23NO2

Guidance literature:

With hydrogen; In ethanol; at 25 - 70 ℃; for 6.5h; under 3878.71 - 7757.43 Torr; Large scale;

DOI:10.1021/op015507o

Reference yield:

(R)-N-[1-(1,3-Benzodioxol-5-yl)butylidene]-α-methylbenzene-methanamine (197508-43-3) → L-694,458 (157341-41-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: hydrogen / ethanol / 6.5 h / 25 - 70 °C / 3878.71 - 7757.43 Torr / Large scale

2.1: acetic acid; palladium 10% on activated carbon; hydrogen / toluene; water; ethanol / 8 h / 20 - 25 °C / 7757.43 Torr / Large scale

2.2: 20 °C / Large scale

3.1: pyridine / toluene / 100 - 110 °C / Large scale

3.2: 106 - 110 °C / Large scale

4.1: lithium tert-butoxide / toluene; hexane / -10 °C / Large scale

With pyridine; palladium 10% on activated carbon; hydrogen; acetic acid; lithium tert-butoxide; In ethanol; hexane; water; toluene;

DOI:10.1021/op015507o

Downstream raw materials:

L-694,458

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