(2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine

Base Information

Chemical Name:(2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine
CAS No.:217298-94-7
Molecular Formula:C₃₅H₃₉NO₄
Molecular Weight:537.699
Hs Code.:

Synonyms:(2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine

Suppliers and Price of (2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine

Chemical Property:

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Technology Process of (2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine

There total 3 articles about (2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: (2R,3R,4R,5R,6S)-1-Benzyl-3,4,5-tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine

: 217298-94-7
(2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine

Guidance literature:: With hydrogen; palladium dihydroxide; In ethanol; ethyl acetate; for 16h; under 2844.3 Torr;
DOI:10.1021/ja960274f

Reference yield:

: 125711-55-9
β-1-C-methyl-deoxymannojirimycin

: 217298-94-7
(2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, -50 deg C, 5 min, 2.) DMF, from 0 deg C to RT, 9 h

2: 96 percent / H₂ / 20percent Pd(OH)2/C / ethyl acetate; ethanol / 16 h / 2844.3 Torr

With hydrogen; sodium hydride; palladium dihydroxide; In ethanol; ethyl acetate;
DOI:10.1021/ja960274f

Reference yield:

: (3R,4S,5S,6R)-6-Azido-1,3,4,5-tetrahydroxy-heptan-2-one

: 217298-94-7
(2R,3R,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-benzyloxymethyl-6-methyl-piperidine

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / H₂ / 10percent Pd/C / methanol / 24 h / 2585.7 Torr

2: 1.) NaH / 1.) DMF, -50 deg C, 5 min, 2.) DMF, from 0 deg C to RT, 9 h

3: 96 percent / H₂ / 20percent Pd(OH)2/C / ethyl acetate; ethanol / 16 h / 2844.3 Torr

With hydrogen; sodium hydride; palladium dihydroxide; palladium on activated charcoal; In methanol; ethanol; ethyl acetate;
DOI:10.1021/ja960274f