methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside

Base Information

Chemical Name:methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside
CAS No.:1315205-95-8
Molecular Formula:C₆₂H₇₁F₃O₁₉S
Molecular Weight:1209.3
Hs Code.:

Synonyms:methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside

Suppliers and Price of methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside

There total 7 articles about methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1315206-39-3
2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-β-D-lactoside

: 1315205-95-8
methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.04.048

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 1315205-95-8
methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 1 h / 70 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

3.1: aluminum (III) chloride; trimethylamine-borane / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: 0.33 h / 20 °C

4.1: pyridine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

With pyridine; aluminum (III) chloride; trimethylamine-borane; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.04.048

Reference yield:

: C₂₁H₃₀O₁₂

: 1315205-95-8
methyl 2,3,6,2',3',6'-hexakis-O-(4-methoxyphenylmethyl)-4'-O-(trifluoromethanesulfonyl)-β-D-lactoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere

2.1: aluminum (III) chloride; trimethylamine-borane / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 0.33 h / 20 °C

3.1: pyridine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

With pyridine; aluminum (III) chloride; trimethylamine-borane; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.04.048