C₆₃H₇₄N₄O₂₁SSi

Base Information

Chemical Name:C₆₃H₇₄N₄O₂₁SSi
CAS No.:204992-96-1
Molecular Formula:C₆₃H₇₄N₄O₂₁SSi
Molecular Weight:1283.45
Hs Code.:

C<sub>63</sub>H<sub>74</sub>N<sub>4</sub>O<sub>21</sub>SSi

Synonyms:C₆₃H₇₄N₄O₂₁SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₆₃H₇₄N₄O₂₁SSi

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Technology Process of C₆₃H₇₄N₄O₂₁SSi

There total 7 articles about C₆₃H₇₄N₄O₂₁SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-24-7
acetic anhydride

: 204992-95-0
C₆₁H₇₂N₄O₂₀SSi

: 204992-96-1
C₆₃H₇₄N₄O₂₁SSi

Guidance literature:: With dmap; In tetrahydrofuran; for 1h; Ambient temperature;
DOI:10.1021/ja9740071

Reference yield:

: 58871-10-6
3,4-di-O-benzyl-D-glucal

: 204992-96-1
C₆₃H₇₄N₄O₂₁SSi

Guidance literature:: Multi-step reaction with 5 steps

1: ZnCl₂ / tetrahydrofuran; diethyl ether

2: 82 percent / collidine, DMAP / 2.5 h / Ambient temperature

3: 83 percent / iodonium bis(sym-collidine) perchlorate, 3 Angstroem molecular sieves / tetrahydrofuran / 0.92 h / -10 - 0 °C

4: 85 percent / tetrabutylammonium azide / tetrahydrofuran / 0.67 h / Ambient temperature

5: 90 percent / DMAP / tetrahydrofuran / 1 h / Ambient temperature

With 2,3,5-trimethyl-pyridine; dmap; iodonium(di-γ-collidine) perchlorate; 3 A molecular sieve; tetrabutylammoniun azide; zinc(II) chloride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja9740071

Reference yield:

: (3aR,4R,7aR)-4-((3aS,4R,6R,7R,7aR)-7-Hydroxy-2-oxo-4-triisopropylsilanyloxymethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxymethyl)-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-2-one

: 204992-96-1
C₆₃H₇₄N₄O₂₁SSi

Guidance literature:: Multi-step reaction with 6 steps

1: dimethyldioxirane / CH₂Cl₂; acetone / 0.5 h

2: ZnCl₂ / tetrahydrofuran; diethyl ether

3: 82 percent / collidine, DMAP / 2.5 h / Ambient temperature

4: 83 percent / iodonium bis(sym-collidine) perchlorate, 3 Angstroem molecular sieves / tetrahydrofuran / 0.92 h / -10 - 0 °C

5: 85 percent / tetrabutylammonium azide / tetrahydrofuran / 0.67 h / Ambient temperature

6: 90 percent / DMAP / tetrahydrofuran / 1 h / Ambient temperature

With 2,3,5-trimethyl-pyridine; dmap; iodonium(di-γ-collidine) perchlorate; 3 A molecular sieve; 3,3-dimethyldioxirane; tetrabutylammoniun azide; zinc(II) chloride; In tetrahydrofuran; diethyl ether; dichloromethane; acetone;
DOI:10.1021/ja9740071