2-((3-(10H-phenothiazin-10-yl)propyl)amino)-2-(4-isopropylphenyl)acetic acid

Base Information

Chemical Name:2-((3-(10H-phenothiazin-10-yl)propyl)amino)-2-(4-isopropylphenyl)acetic acid
CAS No.:1313585-67-9
Molecular Formula:C₂₆H₂₈N₂O₂S
Molecular Weight:432.587
Hs Code.:

Synonyms:2-((3-(10H-phenothiazin-10-yl)propyl)amino)-2-(4-isopropylphenyl)acetic acid

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Chemical Property of 2-((3-(10H-phenothiazin-10-yl)propyl)amino)-2-(4-isopropylphenyl)acetic acid

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Technology Process of 2-((3-(10H-phenothiazin-10-yl)propyl)amino)-2-(4-isopropylphenyl)acetic acid

There total 2 articles about 2-((3-(10H-phenothiazin-10-yl)propyl)amino)-2-(4-isopropylphenyl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313585-66-8
C₄₃H₃₇F₁₇N₂O₃S

: 1313585-67-9
2-((3-(10H-phenothiazin-10-yl)propyl)amino)-2-(4-isopropylphenyl)acetic acid

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In 2,2,3,3-tetrafluoropropanol; at 100 ℃; for 16h; under 2250.23 Torr;
DOI:10.1016/j.tet.2011.05.039

Reference yield:

: 1313585-55-5
N-(3-(10H-phenothiazin-10-yl)propyl)-O-(4-(2-perfluoroctyl-ethyl)benzyl)hydroxylamine hydrochloride

: 16152-51-5
(4-isopropylphenyl)boronic acid

: 1313585-67-9
2-((3-(10H-phenothiazin-10-yl)propyl)amino)-2-(4-isopropylphenyl)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 48 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / 2,2,3,3-tetrafluoropropanol / 16 h / 100 °C / 2250.23 Torr

With palladium 10% on activated carbon; hydrogen; In dichloromethane; 2,2,3,3-tetrafluoropropanol; 1: Petasis reaction;
DOI:10.1016/j.tet.2011.05.039