(3-methoxyl-4-benzyloxyl phenyl)(4-chlorophenyl)methanone

Base Information

Chemical Name:(3-methoxyl-4-benzyloxyl phenyl)(4-chlorophenyl)methanone
CAS No.:134612-27-4
Molecular Formula:C₂₁H₁₇ClO₃
Molecular Weight:352.817
Hs Code.:

Synonyms:(3-methoxyl-4-benzyloxyl phenyl)(4-chlorophenyl)methanone

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Chemical Property of (3-methoxyl-4-benzyloxyl phenyl)(4-chlorophenyl)methanone

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Technology Process of (3-methoxyl-4-benzyloxyl phenyl)(4-chlorophenyl)methanone

There total 2 articles about (3-methoxyl-4-benzyloxyl phenyl)(4-chlorophenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122504-59-0
(3-methoxyl-4-benzyloxyl phenyl)(4-chlorophenyl)methanol

: 134612-27-4
(3-methoxyl-4-benzyloxyl phenyl)(4-chlorophenyl)methanone

Guidance literature:

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 134612-27-4
(3-methoxyl-4-benzyloxyl phenyl)(4-chlorophenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; iodine / tetrahydrofuran / 3.5 h / Inert atmosphere; Reflux

1.2: 4 h / 20 °C / Inert atmosphere

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 4 h / 20 °C

With iodine; magnesium; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1039/c4ob00744a