1-{5-((dimethylamino)methyl)-3-[4-(2-(methoxymethyl)phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-6,6-dimethyl-hepta-2,4-diyn-1-ol

Base Information

Chemical Name:1-{5-((dimethylamino)methyl)-3-[4-(2-(methoxymethyl)phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-6,6-dimethyl-hepta-2,4-diyn-1-ol
CAS No.:1041857-80-0
Molecular Formula:C₂₈H₂₉NO₂S
Molecular Weight:443.61
Hs Code.:

Synonyms:1-{5-((dimethylamino)methyl)-3-[4-(2-(methoxymethyl)phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-6,6-dimethyl-hepta-2,4-diyn-1-ol

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Chemical Property of 1-{5-((dimethylamino)methyl)-3-[4-(2-(methoxymethyl)phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-6,6-dimethyl-hepta-2,4-diyn-1-ol

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Technology Process of 1-{5-((dimethylamino)methyl)-3-[4-(2-(methoxymethyl)phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-6,6-dimethyl-hepta-2,4-diyn-1-ol

There total 1 articles about 1-{5-((dimethylamino)methyl)-3-[4-(2-(methoxymethyl)phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-6,6-dimethyl-hepta-2,4-diyn-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1041857-79-7
C₂₀H₁₉NO₂S

: 84751-19-9
1-trimethylsilyl-4-t-butyl-1,3-butadiyne

: 1041857-80-0
1-{5-((dimethylamino)methyl)-3-[4-(2-(methoxymethyl)phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-6,6-dimethyl-hepta-2,4-diyn-1-ol

Guidance literature:: 1-trimethylsilyl-4-t-butyl-1,3-butadiyne; With methyllithium; In diethyl ether; for 3.5h; Heating;

C₂₀H₁₉NO₂S; In tetrahydrofuran; diethyl ether; at -70 - -55 ℃; for 1.5h; Further stages.;
DOI:10.1016/j.bmc.2008.04.009

Reference yield: 56.0%

: 1041857-80-0
1-{5-((dimethylamino)methyl)-3-[4-(2-(methoxymethyl)phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-6,6-dimethyl-hepta-2,4-diyn-1-ol

: 1041857-69-5
1-{5-((dimethylamino)methyl)-3-[4-(2-(methoxymethyl)phenyl)-buta-1,3-diynyl]-thiophen-2-yl}-6,6-dimethyl-hepta-2,4-diyn-1-one hydrochloride

Guidance literature:: With manganese(IV) oxide; sodium sulfate; In dichloromethane; chloroform; at 0 - 7 ℃; for 16h;
DOI:10.1016/j.bmc.2008.04.009