2-amino-5-phenoxybenzoic acid hydrochloride

Base Information

• Chemical Name: 2-amino-5-phenoxybenzoic acid hydrochloride
• CAS No.: 730980-69-5
• Molecular Formula: C₁₃H₁₁NO₃*ClH
• Molecular Weight: 265.696
• Mol file: 730980-69-5.mol

Synonyms:2-amino-5-phenoxybenzoic acid hydrochloride

Chemical Property of 2-amino-5-phenoxybenzoic acid hydrochloride

Chemical Property:

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Technology Process of 2-amino-5-phenoxybenzoic acid hydrochloride

There total 1 articles about 2-amino-5-phenoxybenzoic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-5-phenoxy-benzoic acid (22071-39-2) → 2-amino-5-phenoxybenzoic acid hydrochloride (730980-69-5)

Guidance literature:

With hydrogenchloride; In diethyl ether; for 2h;

Reference yield: 66.0%

2-amino-5-phenoxybenzoic acid hydrochloride (730980-69-5) + bis(trichloromethyl) carbonate (32315-10-9) → 6-phenoxy-1H-benzo[d][1,3]oxazine-2,4-dione (928029-99-6)

Guidance literature:

With pyridine; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile; at 20 - 55 ℃; for 52.5h;

upstream raw materials:

2-amino-5-phenoxy-benzoic acid

Downstream raw materials:

6-phenoxy-1H-benzo[d][1,3]oxazine-2,4-dione

Refernces