Technology Process of HO2C(C5H3N)CNC6H3(OC8H17)NC6H4C6H5
There total 1 articles about HO2C(C5H3N)CNC6H3(OC8H17)NC6H4C6H5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
formic acid; dihydrogen peroxide;
In
water;
at 0 ℃;
DOI:10.1021/ic100129r
- Guidance literature:
-
With
NaOH;
In
ethanol; water;
aq. NaOH (3 equiv.) added to suspn. of ligand (3 equiv.) in hot EtOH (70-80°C); stirred (10 min); aq. soln. of chloride (1 equiv.) added dropwise over 5 min; stirred (5 min); cooled with stirring (40-50°C); warm filtered; washed (EtOH/H2O, 1/1, hexane); elem. anal.;
DOI:10.1021/ic100129r
- Guidance literature:
-
With
NaOH;
In
ethanol; water;
aq. NaOH (3 equiv.) added to suspn. of ligand (3 equiv.) in hot EtOH (70-80°C); stirred (10 min); aq. soln. of chloride (1 equiv.) added dropwise over 5 min; stirred (5 min); cooled with stirring (40-50°C); warm filtered; washed (EtOH/H2O, 1/1, hexane); elem. anal.;
DOI:10.1021/ic100129r
