Triisopropyl-[(Z)-3-nitro-4-((S)-2-phenyl-[1,3]dioxan-4-yl)-but-3-enyloxy]-silane

Base Information

Chemical Name:Triisopropyl-[(Z)-3-nitro-4-((S)-2-phenyl-[1,3]dioxan-4-yl)-but-3-enyloxy]-silane
CAS No.:482580-57-4
Molecular Formula:C₂₃H₃₇NO₅Si
Molecular Weight:435.636
Hs Code.:

Synonyms:Triisopropyl-[(Z)-3-nitro-4-((S)-2-phenyl-[1,3]dioxan-4-yl)-but-3-enyloxy]-silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Triisopropyl-[(Z)-3-nitro-4-((S)-2-phenyl-[1,3]dioxan-4-yl)-but-3-enyloxy]-silane

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Technology Process of Triisopropyl-[(Z)-3-nitro-4-((S)-2-phenyl-[1,3]dioxan-4-yl)-but-3-enyloxy]-silane

There total 3 articles about Triisopropyl-[(Z)-3-nitro-4-((S)-2-phenyl-[1,3]dioxan-4-yl)-but-3-enyloxy]-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 485800-59-7
2-Nitro-1-((S)-2-phenyl-[1,3]dioxan-4-yl)-4-triisopropylsilanyloxy-butan-1-ol

: 482580-57-4
Triisopropyl-[(Z)-3-nitro-4-((S)-2-phenyl-[1,3]dioxan-4-yl)-but-3-enyloxy]-silane

Guidance literature:: With dicyclohexyl-carbodiimide; copper(l) chloride; In acetonitrile; at 60 ℃; for 15h;
DOI:10.1021/jo020402k

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 482580-57-4
Triisopropyl-[(Z)-3-nitro-4-((S)-2-phenyl-[1,3]dioxan-4-yl)-but-3-enyloxy]-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 2,6-lutidine / CH₂Cl₂ / 1.5 h

2: DBU / acetonitrile / 15 h

3: DCC; CuCl / acetonitrile / 15 h / 60 °C

With 2,6-dimethylpyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; copper(l) chloride; In dichloromethane; acetonitrile; 2: Henry reaction;
DOI:10.1021/jo020402k

Reference yield:

: 482580-71-2
3-nitro-O-triisopropylsilyl-1-propanol

: 482580-57-4
Triisopropyl-[(Z)-3-nitro-4-((S)-2-phenyl-[1,3]dioxan-4-yl)-but-3-enyloxy]-silane

Guidance literature:: Multi-step reaction with 2 steps

1: DBU / acetonitrile / 15 h

2: DCC; CuCl / acetonitrile / 15 h / 60 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; copper(l) chloride; In acetonitrile; 1: Henry reaction;
DOI:10.1021/jo020402k