Bicyclo[6.1.0]non-4-ene-9-carbonyl chloride

Base Information

Chemical Name:Bicyclo[6.1.0]non-4-ene-9-carbonyl chloride
CAS No.:78293-70-6
Molecular Formula:C₁₀H₁₃ClO
Molecular Weight:184.666
Hs Code.:2916209090
DSSTox Substance ID:DTXSID80700859
Mol file:78293-70-6.mol

Synonyms:BICYCLO[6.1.0]NON-4-ENE-9-CARBONYL CHLORIDE;DTXSID80700859

Suppliers and Price of Bicyclo[6.1.0]non-4-ene-9-carbonyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BICYCLO[6.1.0]NON-4-ENE 95.00%
5MG
$ 505.03

Total 3 raw suppliers

Chemical Property of Bicyclo[6.1.0]non-4-ene-9-carbonyl chloride

Chemical Property:

PSA：17.07000
LogP:2.74420
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:184.0654927
Heavy Atom Count:12
Complexity:206

Purity/Quality:

99% ^*data from raw suppliers

BICYCLO[6.1.0]NON-4-ENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2C(C2C(=O)Cl)CCC=C1

Technology Process of Bicyclo[6.1.0]non-4-ene-9-carbonyl chloride

There total 3 articles about Bicyclo[6.1.0]non-4-ene-9-carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 78293-69-3
(Z)-bicyclo[6.1.0]non-4-ene-9-carboxylic acid

: 78293-70-6
(Z)-Bicyclo[6.1.0]non-4-ene-9-carbonyl chloride

Guidance literature:: With thionyl chloride; for 3h;

Reference yield:

: 1552-12-1,111-78-4
1,5-cis,cis-cyclooctadiene

: 78293-70-6
(Z)-Bicyclo[6.1.0]non-4-ene-9-carbonyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 43 percent / copper / cyclohexane / 2 h / 110 °C

2: 98 percent / 10percent aq. sodium hydroxide / ethanol; H₂O / 3 h / Heating

3: 93 percent / thionyl chloride / 3 h

With sodium hydroxide; thionyl chloride; copper; In ethanol; cyclohexane; water;

Reference yield:

: 59891-06-4
7-(ethoxycarbonyl)bicyclo<6.1.0>non-4-ene

: 78293-70-6
(Z)-Bicyclo[6.1.0]non-4-ene-9-carbonyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 10percent aq. sodium hydroxide / ethanol; H₂O / 3 h / Heating

2: 93 percent / thionyl chloride / 3 h

With sodium hydroxide; thionyl chloride; In ethanol; water;