dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside

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Chemical Name:dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside
CAS No.:1115586-43-0
Molecular Formula:C₂₇H₄₃NO₇Si
Molecular Weight:521.726
Hs Code.:

Synonyms:dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside

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Chemical Property of dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside

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Technology Process of dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside

There total 1 articles about dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1115586-42-9
dimethyl t-hexylsilyl 2-acetamido-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside

: 106-95-6
allyl bromide

: 1115586-43-0
dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside

Guidance literature:: dimethyl t-hexylsilyl 2-acetamido-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.166667h; Inert atmosphere;

allyl bromide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.carres.2008.10.007

Reference yield: 70.0%

: 1115586-43-0
dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-4,6-di-O-(4-methoxybenzylidene)-2-deoxy-β-D-glucopyranoside

: 1115586-44-1
dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

: dimethyl t-hexylsilyl 2-acetamido-3-O-allyl-2-deoxy-6-O-(4-methoxybenzyl)-β-D-glucopyranoside

Guidance literature:: With sodium cyanoborohydride; trifluoroacetic acid; In N,N-dimethyl-formamide; at 0 - 20 ℃; Molecular sieve;
DOI:10.1016/j.carres.2008.10.007