pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N^ε-nitro-L-arginine methyl ester

Base Information

Chemical Name:pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N^ε-nitro-L-arginine methyl ester
CAS No.:121191-54-6
Molecular Formula:C₃₃H₄₁N₁₁O₁₄
Molecular Weight:815.754
Hs Code.:

<N-<<6-amino-1-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)-4,5-dihydro-4-oxopyrazolo<3,4-d>pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N<sup>ε</sup>-nitro-L-arginine methyl ester

Synonyms:pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N^ε-nitro-L-arginine methyl ester

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Chemical Property of pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N^ε-nitro-L-arginine methyl ester

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Technology Process of pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N^ε-nitro-L-arginine methyl ester

There total 3 articles about pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N^ε-nitro-L-arginine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 121176-42-9
2',3',5'-tri-O-acetyl-6-azacadeguomycin

: 30668-59-8
L-phenylalaninyl-N^ε-nitro-L-arginine methyl ester trifluoroacetate

: 121191-54-6
pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N^ε-nitro-L-arginine methyl ester

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; 1) 0 deg C, 2) RT;
DOI:10.1021/jm00128a036

Reference yield:

: 108-24-7
acetic anhydride

: 121176-41-8
C₂₇H₃₅N₁₁O₁₁

: 121191-54-6
pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N^ε-nitro-L-arginine methyl ester

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 0 ℃; Yield given;
DOI:10.1021/jm00128a036

Reference yield:

: 96555-48-5
6-azacadeguomycin

: 121191-54-6
pyrimidin-3-yl>carbonyl>-L-phenylalaninyl>-N^ε-nitro-L-arginine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / pyridine / dimethylformamide / 12 h / Ambient temperature

2: 70 percent / 1-hydroxybenzotriazole*H₂O, N-methylmorpholine, 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide*HCl / dimethylformamide; CH₂Cl₂ / 1) 0 deg C, 2) RT

With 4-methyl-morpholine; pyridine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00128a036